水蒸气蒸馏与乙醚超声萃取牡丹皮挥发油的比较研究
投稿时间:2009-12-31  修订日期:2010-04-05  点此下载全文
引用本文:刘职瑞,刘文庸,吴豪,朱臻宇,柴逸峰.水蒸气蒸馏与乙醚超声萃取牡丹皮挥发油的比较研究[J].药学实践杂志,2010,28(4):265~266,270
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作者单位E-mail
刘职瑞 第二军医大学药学院药物分析教研室,上海200433 yfchai@smmu.edu.cn. 
刘文庸 第二军医大学药学院药物分析教研室,上海200433  
吴豪 药明康德新药开发有限公司,上海200131  
朱臻宇 第二军医大学药学院药物分析教研室,上海200433  
柴逸峰 第二军医大学药学院药物分析教研室,上海200433  
基金项目:国家科技支撑计划基金(2006BAI08B03-07);上海市自然科学基金(09dZ1975100)
中文摘要:目的:比较通过不同的提取方法得到的牡丹皮挥发油成分上的差异。方法:分别用水蒸气蒸馏法和乙醚超声萃取法提取牡丹皮挥发油,进行气相-质谱(GC-MS)分析。结果:采用水蒸气蒸馏法挥发油得率为1.2%,被鉴定的成分有17个;乙醚超声萃取法挥发油得率为2.5%,被鉴定的成分有20个。两者共有成分5个。结论:两种提取方法所得牡丹皮挥发油成分存在差异但也有共同特征,乙醚超声萃取法挥发油得率更高,成分更加全面。
中文关键词:牡丹皮  挥发油  水蒸气蒸馏法  乙醚超声萃取法  气相色谱-质谱联用
 
Comparative study on extraction of essential oil from Cortex Moutan by steam distillation and ethyl ether ultrasonic
Abstract:ObjectiveTo compare the difference of essential oil from Cortex Moutan extracted by different method.Methods Steam distillation and ethyl ehter ultrasonic were used to extract the essential oil from Cortex Moutan which were analyzed by GC-MS.Results The extraction rate of essential oil by steam distillation was 1.2%,and 17 compounds were identified.The extraction rate of essential oil by ethyl ehter ultrasonic was 2.5%,and 20 compounds were identified.There were 5 compounds were extracted by both method.Conclusion The essential oil extracted by two Methods have differences but common characteristics in some way.The ethyl ether ultrasonic had higher extraction rate with more chemical constituents.
keywords:Cortex Moutan  essential oil  steam distillation  ethyl ether ultrasonic extraction  GC-MS
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