定氮法测定鱼藤酮辣椒碱悬浮剂中辣椒碱含量
投稿时间:2008-05-19    点此下载全文
引用本文:刘哲鹏,倪德浩,陆丽芳,杨世霆.定氮法测定鱼藤酮辣椒碱悬浮剂中辣椒碱含量[J].药学实践杂志,2009,27(1):43~45
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作者单位
刘哲鹏 上海理工大学医疗器械与食品学院,上海200093 
倪德浩 上海三友生物科技开发有限公司,上海201407 
陆丽芳 上海三友生物科技开发有限公司,上海201407 
杨世霆 上海交通大学药学院,上海200240 
中文摘要:目的:建立鱼藤酮-辣椒碱悬浮剂辣椒碱含量的化学定氮分析方法。方法:定氮法测定悬浮剂中辣椒碱含量。结果用空白对照及蛋白质氮含量进行校正。结果:定氮法测定辣椒碱含量均值为0.25 g/100 mL(精密度RSD1.77%),回收率100.67%(RSD1.65%),蛋白质对辣椒碱含量测定的影响在误差控制范围内。结论:本方法操作简便,重现性好,可作为鱼藤酮-辣椒碱悬浮剂中辣椒碱质量控制方法。
中文关键词:定氮法  鱼藤酮-辣椒碱悬浮剂  含量测定
 
Determination of capsaicin in rotenone-capsaicin suspension by nitrogen determination method
Abstract:Objective: To establish a nitrogen determination method for determining capsaicin in rotenone-capsaicin suspension.Methods: The capsaicin of suspension was determined by the nitrogen determination method.The results were regulated by blank control and protein control.Results:The content in suspension was 0.25 g/100 mL and RSD was 1.77%.The mean average recovery of the method was 100.67% and RSD was 1.65%.The error of the protein influence was in control.Conclusion:The method was simple and accurate.It could be used to quality control of the rotenone-capsaicin suspension.
keywords:nitrogen determination method  rotenone-capsaicin suspension  determination of content
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