| 碳糊电极阳极吸附伏安法测定雷贝拉唑 |
| 投稿时间：2007-12-11 修订日期：2007-01-15 点此下载全文 |
| 引用本文：郭利民,钟世华,李伟,黄叶菊.碳糊电极阳极吸附伏安法测定雷贝拉唑[J].药学实践杂志,2008,(1):35~37 |
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| 中文摘要:目的:建立测定雷贝拉唑含量的新方法。方法:采用碳糊电极阳极吸附伏安法,在1.8mol/L H2SO4底液中,通过富集用碳糊电极阳极吸附伏安法研究雷贝拉唑的电化学行为。结果:阳极峰电位为0.498V（vs.SCE）,峰电流与雷贝拉唑的浓度在4.15×10-7-3.37×10-6mol/L范围内呈良好的线性关系,检出限为6.705×10-11mol/L。结论:本方法简便准确,适用于雷贝拉唑的含量测定。 |
| 中文关键词:雷贝拉唑 碳糊电极 阳极吸附伏安法 |
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| Determination of rabeprazole at a carbon paste electrode by anodic adsorptive voltammetry |
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| Abstract:Objective:To establish a new method for the determination of rabeprazole.Methods: Anodic adsorptive voltammetry with a carbon paste electeode(CPE) was used. Rabeprazole was concentrated on the electrode and determined by adsorptive voltammetry in supporting solution of 1.8 mol/L H2SO4.Results:The anthodic peak potential of raberazole was at 0.498 V(vs.SCE). The peak currents were linear with the concentration of rabeprazole over the range of 4.15×10-7～3.73×10--6mol/L, with the detection limit 6.705×10--11 mol/L. Conclusion: This method is suitable for the determination of rabeprazole, and it is covenient and accurate. |
| keywords:rabeprazole canbon paste etectrode anodic adsorptive voltammetry |
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