康肾丸质量控制的研究
投稿时间:2007-02-09    点此下载全文
引用本文:闫冰,陆晓和,魏群利,夏曙辉.康肾丸质量控制的研究[J].药学实践杂志,2007,(4):219~221,237
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作者单位
闫冰 南京军区南京总医院制剂科,江苏南京210002 
陆晓和 南京军区南京总医院制剂科,江苏南京210002 
魏群利 南京军区南京总医院制剂科,江苏南京210002 
夏曙辉 南京军区南京总医院制剂科,江苏南京210002 
中文摘要:目的:建立康肾丸的质量控制方法。方法:采用薄层色谱法(TLC)对方中主要药材黄芪、虫草菌丝粉、防风分别进行定性鉴别;采用高效液相色谱法(HPLC)测定黄芪甲苷的含量。结果:定性鉴别方法重现性好,专属性强;含量测定的加样回收率为99.39%,RSD为0.59%。结论:本方法简单、易行、精密度高、重复性好,能够有效地控制康肾丸的质量。
中文关键词:康肾丸  薄层色谱法  黄芪甲苷  高效液相色谱法
 
Studies on quality control of Kangshen pills
Abstract:Objective:To establish a method for quality control of Kangshen pills.Methods:The qualitative analysis of Radix As- tragali,mycelium powder of Cordyceps Sinrnsis,Radix Saposhnikoviae in Kangshen pills were identified by TLC.The content of astra- galosideⅣwas determinated by HPLC.Results:Methods of the qualitative identification were specific and reproducible.The average recovery was 99.39% and relative standard deviation was 0.59%.Conclusion:The precision and reproducibility of the method were good.The method can be used for quality control of Kangshen pills.
keywords:Kangshen pill  TLC  astragalosideⅣ  HPLC
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