青钱柳水溶性成分的研究
投稿时间:2007-01-19    点此下载全文
引用本文:张娟,路金才,肖凯,吕挺,樊军文,张黎明,赵杰,杨建军.青钱柳水溶性成分的研究[J].药学实践杂志,2007,(2):82~84
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作者单位E-mail
张娟 第二军医大学海军医学系毒物药物研究室,上海200433
沈阳药科大学中药学院,辽宁 沈阳110016 
Kaixiaocn@gmail.com 
路金才 沈阳药科大学中药学院,辽宁 沈阳110016  
肖凯 第二军医大学海军医学系毒物药物研究室,上海200433  
吕挺 第二军医大学海军医学系毒物药物研究室,上海200433  
樊军文 第二军医大学海军医学系毒物药物研究室,上海200433  
张黎明 第二军医大学海军医学系毒物药物研究室,上海200433  
赵杰 第二军医大学海军医学系毒物药物研究室,上海200433  
杨建军 江西九江绿色产业发展有限公司,江西 修水332400  
基金项目:国家自然科学基金(30472141);上海-SK研究与发展基金(2004005-t)
中文摘要:目的:研究青钱柳的水溶性成分。方法:利用反相色谱的方法分离纯化,根据化合物的化学性质与光谱数据鉴定结构。结果:青钱柳的70%乙醇提取物中分得7个化合物,确定其结构分别为山奈酚-3-O-β-D-吡喃葡萄糖醛酸钠盐(kaempferol-3-O-β-D-glucuronate sodium,Ⅰ)、槲皮素-3-O-β-D-葡萄糖醛酸钠盐(quer-eetin-3-O-β-D-glucuronate sodium,Ⅱ)、杨梅素-3-Oβ-D-葡萄糖醛酸钠盐(myricetin-3-O-β-D-glucuronate sodi-um,Ⅲ)、2,6-二甲氧基-4-羟基苯酚-1-O-β-D-吡喃葡萄糖苷(2,6-dimethoxy-4-hydroxyphenol-1-O-β-D-gluco-pyranoside,Ⅳ)、色氨酸(tryptophan,Ⅴ)、没食子酸(gallic acid,Ⅵ),苯甲酸(benzoic acid,Ⅶ)。结论:化合物Ⅰ~Ⅵ为首次从该属中分得。
中文关键词:青钱柳  水溶性成分
 
Studies on water-soluble constituents in the leaves of Cyclocarya paliurus
Abstract:Objective:To study the water-soluble constituents from Cyclocarya paliurus(Batal)Ijinskaja Methods:The constitu-ents were isolated by reverse-phased materials,and their structures were characterized by chemical property and spectral analysis.Results:Seven compounds were isolated from the 70% ethanol extract of the leaves of Cyclocarya paliurus.Their structures were elucida-ted as kaempferol-3-O-β-D-glucuronate sodium(Ⅰ),quercetin-3-O-β-D-glucuronate sodium(Ⅱ),myricetin-3-O-β-D-glucuronate so-dium (Ⅲ),2,6-dimethoxy-4-hydroxyphenol-1-O-β-D-glucopyranoside(Ⅳ),tryptophan(Ⅴ),gallic acid(Ⅵ)and benzoic acid (Ⅶ)respectively.Conclusion:CompoundsⅠ~Ⅵare isolated from this genus for the first time.
keywords:Cyclocary paliurus  water-soluble chemical constituents
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