| 测定通脉灵片中丹参素含量 |
| 投稿时间：2006-04-03 点此下载全文 |
| 引用本文：邢军,李正国,张中湖.测定通脉灵片中丹参素含量[J].药学实践杂志,2007,(1):35~37 |
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| 中文摘要:目的:建立通脉灵片中丹参素的含量测定方法。方法:采用KromasilTM C18柱（200 mm×4．6 mm,5μm ）,流动相为甲醇-乙腈-0．045 mol/L磷酸溶液（10:4:86）,检测波长281 nm。结果:丹参素的线性范围为0．194～2．129μg,r=0．999 8。平均加样回收率为99．56％,RSD为0．84％（n=5）。结论:该方法灵敏、简便、重现性好,可用于该制剂的质量控制。 |
| 中文关键词:通脉灵片 丹参素 高效液相色谱法 |
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| Determination of the przewatanshinquinone in Tongmailing tabeles |
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| Abstract:Objective:To establish a HPLC method of the determination of the przewatanshinquinone in Tongmailing tabeles. Methods:The determination was performed by Re-HPLC on KromasilTM C18 column（200 mm×4.6 mm,5μm）using methanol-toni- trile-0.045 mol/L H3 PO4（10:4:86）as mobile phase,the detection wavelength was 281 nm.Results:The linear rang of przewatan- shinquinone was 0.194～2.129μg,r=0.999 8.The average recovery was 99.56%,RSD was 0.84%（n=5）.Conclusion:The method is sensitive,simple,and good reproducibility,which can be applied to the quality control of the preparation. |
| keywords:Tongmailing tabeles przewatanshinquinone HPLC |
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