| 高效液相色谱法测定百年康口服液中橙皮苷的含量 |
| 投稿时间：2006-03-21 点此下载全文 |
| 引用本文：叶光明,瞿发林,刘桂永,谈丽娜,蒋勤,赵勇.高效液相色谱法测定百年康口服液中橙皮苷的含量[J].药学实践杂志,2006,(5):293~295 |
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| 中文摘要:目的：建立百年康口服液中橙皮苷的含量测定方法。方法：采用HPLC法, 色谱柱为YWG C18（150mm×4．6mm, 5μm）, 流动相为乙腈-0．25%磷酸水（20∶80）；检测波长为285nm, 流速为1．0mL/min。结果：橙皮苷在5～50mg/L浓度范围内呈良好的线性关系（r=0．9996）, 平均回收率为100．92%, RSD为1．78%。结论：本法灵敏、准确、重现性好、精密度高、专属性强, 可用于百年康口服液中橙皮苷的含量测定和质量控制。 |
| 中文关键词:橙皮苷 高效液相色谱法 百年康口服液 |
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| Determination of hesperidin in Bainiankang oral liquid by HPLC |
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| Abstract:Objective:To establish the determination of hesperidin in Bainiankang oral liquid.Methods:The determination was car-ried out by HPLC with a YWG C18（150mm×4.6mm, 5μm）column, acetonitrile-0.25% water（20:80）as mobile phase, detection wavelength was at 285nm, flow rate was 1.0 mL/min.Results:Hesperidin showed a good linear relationship at the range of 5～50mg/L, r=0.999 6.The average recovery was 100.92% and RSD was 1.78%.Conclusion:The method is sensitive, accurate, re-producible, specific and can be used for quality control of Bainiankang oral liquid. |
| keywords:Hesperidin HPLC Bainiankang Oral Liquid |
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