| 高效离子对液相色谱法测定促甲状腺激素释放激素(TRH)血药浓度的研究 |
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| 引用本文：柳正良,李名秀,崔志平.高效离子对液相色谱法测定促甲状腺激素释放激素(TRH)血药浓度的研究[J].药学实践杂志,1995,(4):234~236 |
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| 中文摘要:报告反相离子对高效液相色谱法测定兔血浆中促甲状腺激素释放激素(TRH)的浓度。采用ODS色谱柱,流动相为0.02NHAC:乙腈:庚烷磺酸(89.85:10:0.15),流速1.5ml/min,检测波长为220nm.平均回收率101.69%,RSD为1.28%.本法操作简便,结果准确,重现性好。 |
| 中文关键词:离子对 高效液相色谱 促甲状腺激素释放激素(TRH) 血药浓度 |
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| The determination of thyotropin-releasing hormone in plasma by ion pair Rp-HPLC |
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| Abstract:The method for the determination of Thyrotropin-Releasing Hormore in plasma by ion pair RP-HPLC was studied.(column:ODS:mobile phase:0.02mol/1.HAC-acetonitril-sodium 1-heptanesulfonate (89.85:10:0.15):flow rate:1.5ml/min detector:UV 220nm,0.1UFS.The average recovery was 101.69 ± 1.31%. The relation coefficient reached 0.9998.The method was simple and gave correct result and better reproducibility. |
| keywords:ION pair RP-HPLC thyrotropin-releasing hormone plasma concentration |
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